4,5-Dimethoxy-2-(4-methylbenzoyl)-1-(4-methylphenylsulfonylamido)benzene

[2,7-Dimethoxy-8-(4-methylbenzoyl)-1-naphthyl](4-methylphenyl)methanone

In the title compound, C(28)H(24)O(4), the two 4-methyl-benzoyl groups at the 1- and 8-positions of the naphthalene ring system are aligned almost anti-parallel, the dihedral angle between the two phenyl rings being 9.64 (7)°. The dihedral angles between the two phenyl rings and the naphthalene ring system are 71.82 (6) and 71.58 (6)°. In the crystal, inter-molecular C-H⋯O inter-actions between...

[2-(4-Methylbenzoyl)phenyl](4-methylphenyl)methanone

The asymmetric unit of the title compound, C(22)H(18)O(2), contains one half-mol-ecule, the complete mol-ecule being generated by the operation of a crystallographic twofold rotation axis. The carbonyl group and the two C atoms attached to it forms inter-planar angles of 23.67 (7)° with the methyl-substituted phenyl ring and 50.74 (8)° with the central ring. In the crystal, mol-ecules are linke...

1 - Fluoro - 2 , 5 - dimethoxy - 4 - nitrobenzene

1-Fluoro-2,5-dimethoxy-4-nitrobenzene was synthesized in 90% yield by the reaction of commercial 2-fluoro-1,4-dimethoxybenzene with nitric acid. The structure was confirmed by X-ray crystallography. The new title compound was characterized by 1H and 13C-NMR, elemental analysis, EI-MS and FT-IR.

1 , 4 - Phenylenebis [ ( 6 , 7 - dimethoxy - 3 , 4 - dihydroisoquinolin - 2 ( 1 H ) - yl ) methanone ]

The compound named in the title was prepared from N1,N4-diphenethylterephthalamide 1. The resulting bis terephthalamide was subjected to an intramolecular α-amidoalkylation reaction with paraformaldehyde in the presence of heterogeneous catalyst TfOH/SiO2 to obtain 1,4-phenylenebis[(6,7-dimethoxy-3,4-dihydroisoquinolin-2(1H)-yl)methanone]. The structure of the newly synthesized compound was det...

Analogs of amphetamine. 6. 2,5-Dimethoxy-4-methyl- and 2,5-dimethoxy-alpha,4-dimethylphenylalanines.